Once in a while, you may run into this problem,the experiment fails at atm either on 600 or 400. Do the following:
a). Stop the automation in IconNMR. Most of the time it will prompt you to change to another user before you can stop the automation. Follow the instructions on the pop-up window.
b). In Topspin window, type ii. Run ii a few times until you see no error messages. Then you can try atma and see if it works here(Better yet, you can manually tune and match the probe after typing in atmm.). If it finishes without errors, you can go back to iconnmr to restart the automation.
c). If running ii keeps on returning errors, you will need to restart Topspin.
On Fourier 300MHz, it will ask you to update the field once in a while. This is done under edlock's BSMS tap. On other Bruker spectrometers, if the field dirfts so far off that you cannot lock the spectrometer, it calls for changing the base frequency. After that, expinstall all pulse sequences and parameter sets.
On Aglient 500MHz spectrometer,in the same study in walkup account you will need to run all 1D spectra before you run 2Ds, otherwise, a 1D and other followed experiments after a 2D will not run.
How to edit other acquisition parameters not shown in IconNMR?Click on "Edit all Acquisition Parameters" to go to Topspin interface.
You can either edit parameters here or click on the square pulse shape button to go to another page which shows pulse program parameters only(recommended). After editting all necessary parameters, you'll need to click on "Return to IconNMR" to go back to IconNMR interface. DO NOT change the power levels unless you know what you are doing.
The good starting shim called LASTBEST was generated by Xu in all Bruker spectrometers. DO NOT mess with that. You read the starting shim by typing in "rsh"