NMR SPECTROMETERS

• Varian VNMRS 500 MHz Nuclear Magnetic Resonance Spectrometer, with Z-gradients, fully multinuclear (autotune probe) and equipped for continuous variable temperature operation
• Bruker AMX 360 MHz, multi-nuclear (¹H, ¹³C, ³¹P, ¹¹B), variable temperature
• Bruker DPX 300 MHz, multi-nuclear (¹H, ¹³C, 19F, ³¹P)

MASS SPECTROMETERS

• Thermo Orbitrap (ESI and APCI/APPI ionizations, HRMS up to 30,000)
• Waters Synapt LC-MS (ESI ionization, HRMS up to 17,000)
• Waters Prospec 3000 (EI and CI ionizations, HRMS up to 10,000)
• Thermo LCQ (ESI ionization, 2000 AMU)
• Thermo DSQ GC/MS with solids probe (EI ionization, 1050 AMU)

X-RAY DIFFRACTOMETER

• Bruker CCD single-crystal diffractometer with low temperature

ORD/CD

• JASCO Model J-810 Spectropolarimeter with six position Peltier thermoelectric control system

POLARIMETER

• Rudolph Autopol automatic polarimeter

CALORIMETERS

• Microcal ITC-200 micro isothermal titration calorimeter
• Calorimetry Services Corporation Isothermal Titration Calorimeter

In addition, the department has numerous UV-vis and IR spectrometers, gas and liquid chromatographs and fluorimeters, a UV reactor and a spinning band distillation apparatus.